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Tutorial for Relaxation dispersion analysis cpmg fixed time recorded on varian as fid interleaved

708 bytes added, 08:51, 27 August 2013

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gedit ../peak_lists/peaks_corr_final.list &

</source>

Then alter to:

H30N-HN 117.794 8.045

A57N-HN 121.417 7.944

D68N-HN 121.402 7.922

Then check again in sparky.

== Check for peak movement ==

As stated in the [[manual || relax manual]] section '''5.2.1 Temperature control and calibration''', the pulse sequence can put a lot of power into the sample. <br>

It is therefore good practice to inspect for peak movements, by overlaying all spectra:

Open all the files, and overlay them with SPARKY command '''ol'''.

sparky 0.fid/test.ucsf 1.fid/test.ucsf 2.fid/test.ucsf 3.fid/test.ucsf 4.fid/test.ucsf

</source>

Changes colours for different spectra in contour '''ct'''.<br>

Then overlay with "ol". Make sure no peaks move around.

= See also =

[[Category:Tutorials]]

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